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Title: Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
Author: Katsikis, Sotirios
Marín Montesinos, Ildefonso
Pons Vallès, Miquel
Ludwig, Christian
Günther, Ulrich L.
Keywords: Espectroscòpia de ressonància magnètica nuclear
Polarització (Física nuclear)
Nuclear magnetic resonance spectroscopy
Polarization (Nuclear physics)
Issue Date: 26-Jul-2015
Publisher: Springer Verlag
Abstract: Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system.
Note: Versió postprint del document publicat a:
It is part of: Applied Magnetic Resonance, 2015, vol. 46, num. 7, p. 723-729
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ISSN: 0937-9347
Appears in Collections:Publicacions de projectes de recerca finançats per la UE
Articles publicats en revistes (Química Inorgànica i Orgànica)

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