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http://hdl.handle.net/2445/138570
Title: | Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device |
Author: | Katsikis, Sotirios Marín Montesinos, Ildefonso Pons Vallès, Miquel Ludwig, Christian Günther, Ulrich L. |
Keywords: | Espectroscòpia de ressonància magnètica nuclear Polarització (Física nuclear) Nuclear magnetic resonance spectroscopy Polarization (Nuclear physics) |
Issue Date: | 26-Jul-2015 |
Publisher: | Springer Verlag |
Abstract: | Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system. |
Note: | Versió postprint del document publicat a: https://doi.org/10.1007/s00723-015-0680-5 |
It is part of: | Applied Magnetic Resonance, 2015, vol. 46, num. 7, p. 723-729 |
URI: | http://hdl.handle.net/2445/138570 |
Related resource: | https://doi.org/10.1007/s00723-015-0680-5 |
ISSN: | 0937-9347 |
Appears in Collections: | Articles publicats en revistes (Química Inorgànica i Orgànica) Publicacions de projectes de recerca finançats per la UE |
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655715.pdf | 962.54 kB | Adobe PDF | View/Open |
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