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Si us plau utilitzeu sempre aquest identificador per citar o enllaçar aquest document: https://hdl.handle.net/2445/48635

Convergent Approaches for the Synthesis of the Anti-tumoral Peptide, Kahalalide F. Study of Orthogonal Protecting Groups

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Kahalalide compounds are peptides that are isolated from a Hawaiian herbivorous marine species of mollusc, Elysia rufescens, and its diet, the green alga Bryopsis sp. Kahalalide F and its synthetic analogues are the most promising compounds of the Kahalalide family because they show anti-tumoral activity. Linear solid-phase syntheses of Kahalalide F have been reported. Here we describe several new improved synthetic routes based on convergent approaches with distinct orthogonal protection schemes for the preparation of Kahaladide analogues. These strategies allow a better control and characterization of the intermediates because more reactions are performed in solution. Five derivatives of Kahalalide F were synthesized using several convergent approaches.

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GRACIA, Carolina, ISIDRO LLOBET, Albert, CRUZ, Luis j., ACOSTA, Gerardo a., ÁLVAREZ DOMINGO, Mercedes, CUEVAS, Carmen, GIRALT LLEDÓ, Ernest, ALBERICIO PALOMERA, Fernando. Convergent Approaches for the Synthesis of the Anti-tumoral Peptide, Kahalalide F. Study of Orthogonal Protecting Groups. _Journal of Organic Chemistry_. 2006. Vol. 71, núm. 7196. [consulta: 5 de desembre de 2025]. ISSN: 0022-3263. [Disponible a: https://hdl.handle.net/2445/48635]

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