Microwave assisted synthesis of polynuclear Ni(II) complexes

Rosado Piquer, LidiaSañudo Zotes, Eva Carolina2019-09-062021-05-122019-05-120277-5387https://hdl.handle.net/2445/139420In this paper we test a solvent-free microwave assisted synthesis method with a known Ni7 complex, [Ni7(chp)12(OH)2(CH3OH)6] (2), and then extended the method to a more complex ligand system. We prepare two new trinuclear Ni(II) complexes ([Ni3(chp)4(tBuSALOH)2(MeOH)5] (4) and [Ni3(chp)4(iPrSALOH)2(MeOH)6] (5)) and report here their characterization and magnetic properties.7 p.application/pdfengcc-by-nc-nd (c) Elsevier Ltd, 2019http://creativecommons.org/licenses/by-nc-nd/3.0/esComplexos metàl·licsPropietats magnètiquesMetal complexesMagnetic propertiesMicrowave assisted synthesis of polynuclear Ni(II) complexesinfo:eu-repo/semantics/article6911422019-09-06info:eu-repo/semantics/openAccess