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http://hdl.handle.net/2445/176670| Title: | Electron energy-loss spectroscopic tomography of FexCo(3-x)O4 impregnated Co3O4 mesoporous particles: unraveling the chemical information in three dimensions |
| Author: | Yedra Cardona, Lluís Eljarrat Ascunce, Alberto Arenal, Raúl López Conesa, Lluís Pellicer Vilà, Eva M. López-Ortega, Alberto Estrader i Bofarull, Marta Sort, Jordi Baró, M. D. Estradé Albiol, Sònia Peiró Martínez, Francisca |
| Keywords: | Tomografia Espectroscòpia de pèrdua d'energia d'electrons Nanoestructures Tomography Electron energy loss spectroscopy Nanostructures |
| Issue Date: | 1-Jan-2016 |
| Publisher: | Royal Society of Chemistry |
| Abstract: | Electron energy-loss spectroscopy-spectrum image (EELS-SI) tomography is a powerful tool to investigate the three dimensional chemical configuration in nanostructures. Here, we demonstrate, for the first time, the possibility to characterize the spatial distribution of Fe and Co cations in a complex FexCo(3-x)O4/Co3O4 ordered mesoporous system. This hybrid material is relevant because of the ferrimagnetic/antiferromagnetic coupling and high surface area. We unambiguously prove that the EELS-SI tomography shows a sufficiently high resolution to simultaneously unravel the pore structure and the chemical signal. |
| Note: | Versió postprint del document publicat a: https://doi.org/10.1039/c6an00562d |
| It is part of: | Analyst, 2016, vol. 141, num. 16, p. 4968-4972 |
| URI: | http://hdl.handle.net/2445/176670 |
| Related resource: | https://doi.org/10.1039/c6an00562d |
| ISSN: | 0003-2654 |
| Appears in Collections: | Articles publicats en revistes (Química Inorgànica i Orgànica) Articles publicats en revistes (Enginyeria Electrònica i Biomèdica) |
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| File | Description | Size | Format | |
|---|---|---|---|---|
| 668285.pdf | 1.03 MB | Adobe PDF | View/Open |
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