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X-ray diffraction pattern analysis of CrFeCoNi high-entropy alloy deposited via cold spray
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CrFeCoNi high-entropy alloy (HEA) powder with an equimolar composition was produced via gas atomization and applied as a coating using the cold-spray technique. X-ray diffraction patterns were analyzed to characterize the microstructure of the raw HEA powder and cold-sprayed coatings using Rietveld refinement methods. The HEA powders exhibited a single-phase face-centered cubic crystal structure with a lattice parameter of 0.357349(1) nm, a low microstrain of 4.3(0.17) × 10−4, and a crystallite size of 225(8) nm, attributed to the rapid cooling during atomization. In contrast, the cold-sprayed coatings exhibited broadened diffraction peaks, with a reduced crystallite size of 67.9(1.2) nm and an increased microstrain of 2.2(0.23) × 10−3, showing crystallite size refinement and an increase in the density of crystalline defects due to severe plastic deformation during deposition. Additional microstructural analysis revealed texture in the {200} plane and intrinsic stacking fault probabilities increasing to 4.4(0.21) × 10−3. These findings highlight microstructural changes produced by the cold-spray process. This study provides valuable insights into optimizing cold-spray parameters and tailoring HEA properties for industrial applications.
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SILVELLO, A. (Alessio), et al. X-ray diffraction pattern analysis of CrFeCoNi high-entropy alloy deposited via cold spray. Powder Diffraction. 2025. Vol. 40, num. 4, pags. 269-278. ISSN 0885-7156. [consulted: 25 of May of 2026]. Available at: https://hdl.handle.net/2445/228311