Scalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals

dc.contributor.authorShavel, Alexey
dc.contributor.authorIbáñez Sabaté, Maria
dc.contributor.authorLuo, Zhishan
dc.contributor.authorDe Roo, Jonathan
dc.contributor.authorCarreté, Àlex
dc.contributor.authorDimitrievska, Mirjana
dc.contributor.authorGenç, Aziz
dc.contributor.authorMeyns, Michael
dc.contributor.authorPérez Rodríguez, Alejandro
dc.contributor.authorKovalenko, Maksym V.
dc.contributor.authorArbiol i Cobos, Jordi
dc.contributor.authorCabot i Codina, Andreu
dc.date.accessioned2018-10-04T16:21:20Z
dc.date.available2018-10-04T16:21:20Z
dc.date.issued2016
dc.date.updated2018-10-04T16:21:20Z
dc.description.abstractMonodisperse Cu2ZnSnS4 (CZTS) nanocrystals (NCs), with quasi-spherical shape, were prepared by a facile, high-yield, scalable, and high-concentration heat-up procedure. The key parameters to minimize the NC size distribution were efficient mixing and heat transfer in the reaction mixture through intensive argon bubbling and improved control of the heating ramp stability. Optimized synthetic conditions allowed the production of several grams of highly monodisperse CZTS NCs per batch, with up to 5 wt % concentration in a crude solution and a yield above 90%.
dc.format.extent7 p.
dc.format.mimetypeapplication/pdf
dc.identifier.idgrec660689
dc.identifier.issn0897-4756
dc.identifier.urihttps://hdl.handle.net/2445/125077
dc.language.isoeng
dc.publisherAmerican Chemical Society
dc.relation.isformatofVersió postprint del document publicat a: https://doi.org/10.1021/acs.chemmater.5b03417
dc.relation.ispartofChemistry of Materials, 2016, vol. 28, num. 3, p. 720-726
dc.relation.projectIDinfo:eu-repo/grantAgreement/EC/FP7/284486/EU//SCALENANO
dc.relation.projectIDinfo:eu-repo/grantAgreement/EC/FP7/306733/EU//NANOSOLID
dc.relation.projectIDinfo:eu-repo/grantAgreement/EC/FP7/316488/EU//KESTCELLS
dc.relation.projectIDinfo:eu-repo/grantAgreement/EC/FP7/310250/EU//UNION
dc.relation.urihttps://doi.org/10.1021/acs.chemmater.5b03417
dc.rights(c) American Chemical Society , 2016
dc.rights.accessRightsinfo:eu-repo/semantics/openAccess
dc.sourceArticles publicats en revistes (Enginyeria Electrònica i Biomèdica)
dc.subject.classificationQuímica de superfícies
dc.subject.classificationNanocristalls
dc.subject.classificationNanopartícules
dc.subject.classificationTermoelectricitat
dc.subject.otherSurface chemistry
dc.subject.otherNanocrystals
dc.subject.otherNanoparticles
dc.subject.otherThermoelectricity
dc.titleScalable heating-up synthesis of monodisperse Cu2ZnSnS4 nanocrystals
dc.typeinfo:eu-repo/semantics/article
dc.typeinfo:eu-repo/semantics/acceptedVersion

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