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2025-08

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cc-by (c) Núñez et al., 2025
Si us plau utilitzeu sempre aquest identificador per citar o enllaçar aquest document: https://hdl.handle.net/2445/223312

An FIA-MS Method for Rapid Coffee Adulteration Detection: A Comparative Study with a Non-Targeted LC-MS Approach

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Recurs relacionat

https://doi.org/https://doi.org/10.3390/foods14172931

Resum

Coffee adulteration is a growing concern in the food industry due to economic and quality implications. This study evaluates a rapid, non-targeted fingerprinting method based on flow injection analysis–mass spectrometry (FIA-MS) for detecting common coffee adulterants. A total of 119 samples were analyzed, including 43 coffee samples and 76 samples of common coffee adulterants (16 chicory, 10 barley, and 50 flour samples). FIA-MS combined with chemometric analysis allowed for the classification of pure and adulterated coffee samples with over 95% accuracy. Compared to LC-MS, the FIA-MS method showed a similar performance while offering significantly faster analysis and lower solvent consumption, making it a practical and sustainable option for high-throughput screening. For PLS regression studies, calibration and prediction errors were consistently below 0.91% and 11.7%, respectively. Furthermore, the methodology was compared with a non-targeted LC-MS approach, showing an excellent performance.

Matèries

Anàlisi per injecció en flux, Cafè (Beguda), Quimiometria

Matèries (anglès)

Flow injection analysis, Coffee drink, Chemometrics

Citació

Col·leccions

Articles publicats en revistes (Enginyeria Química i Química Analítica)

Citació

NÚÑEZ BURCIO, Oscar, NÚÑEZ, Nerea and SAURINA, Javier. An FIA-MS Method for Rapid Coffee Adulteration Detection: A Comparative Study with a Non-Targeted LC-MS Approach. Foods. 2025. Vol. 14, num. 2391. ISSN 2304-8158. [consulted: 18 of August of 2026]. Available at: https://hdl.handle.net/2445/223312

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