Solvent-controlled diastereoselectivity in tryptophan-catalyzed Mannich reactions

dc.contributor.authorValero González, Guillem
dc.contributor.authorLeón, Carlos M.
dc.contributor.authorMoyano i Baldoire, Albert
dc.date.accessioned2018-02-19T11:19:17Z
dc.date.available2018-02-19T11:19:17Z
dc.date.issued2015-06-12
dc.date.updated2018-02-19T11:19:17Z
dc.description.abstractSolvent effects in the L-tryptophan-catalyzed Mannich reaction between hydroxyacetone and glyoxylate imines have been examined. The use of a DMSO/1-butanol (4:1 v/v) mixture as solvent at rt provided the expected Mannich adducts in good yields, high anti-diastereoselectivity (up to 10.3:1 anti/syn ratio) and excellent enantioselectivities (up to >99.9% ee for the anti isomer)
dc.format.extent10 p.
dc.format.mimetypeapplication/pdf
dc.identifier.idgrec668850
dc.identifier.issn2300-4630
dc.identifier.urihttps://hdl.handle.net/2445/119967
dc.language.isoeng
dc.publisherDe Gruyter Open
dc.relation.isformatofhttps://doi.org/10.1515/asorg-2015-0001
dc.relation.ispartofAsymmetric Catalysis, 2015, vol. 2, num. 1, p. 7-16
dc.relation.urihttps://doi.org/10.1515/asorg-2015-0001
dc.rightscc by-nc-nd (c) Valero González, Guillem et al., 2015
dc.rights.accessRightsinfo:eu-repo/semantics/openAccess
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/3.0/es/
dc.sourceArticles publicats en revistes (Química Inorgànica i Orgànica)
dc.subject.classificationAminoàcids
dc.subject.classificationCatàlisi asimètrica
dc.subject.otherAmino acids
dc.subject.otherEnantioselective catalysis
dc.titleSolvent-controlled diastereoselectivity in tryptophan-catalyzed Mannich reactions
dc.typeinfo:eu-repo/semantics/article
dc.typeinfo:eu-repo/semantics/publishedVersion

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