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Synthesis, Structural Characterization and Spectroscopic Properties of 1,2-Bis[4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-oxobutyl]benzene

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dc.contributor.authorGuerrero, Miguel
dc.contributor.authorPons, Josefina
dc.contributor.authorFont Bardia, Ma. Mercedes
dc.contributor.authorCalvet Pallàs, Maria Teresa
dc.contributor.authorRos, Josep
dc.date.accessioned2024-06-17T06:21:59Z
dc.date.available2024-06-17T06:21:59Z
dc.date.issued2011-01-31
dc.date.updated2024-06-17T06:22:05Z
dc.description.abstractThe crystal structure of the title compound C22H30N4O2 H2O (L), has been determined using X-ray diffraction at 293 K. The crystal of 1,2-bis[4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-oxobutyl]benzene is in triclinic crystal system with space group P(-1) (Z = 2), lattice parameters a = 8.225(6) A ° , b= 10.967(6) A ° , c=12.903(6) A ° , V = 1119.1(11) A ° 3. Analyses of single crystals of L, crystallized from dichloromethane/diethyl ether (1:1), revealed that the molecules are arranged in couples, which adopt a pseudo chair conformation, by means of intermolecular O-H N hydrogen bonding interactions. Moreover, the extended structure revealed a 1D chain caused by several C-H N intermolecular interactions.
dc.format.extent20 p.
dc.format.mimetypeapplication/pdf
dc.identifier.idgrec600141
dc.identifier.issn1074-1542
dc.identifier.urihttps://hdl.handle.net/2445/213300
dc.language.isoeng
dc.publisherSpringer Verlag
dc.relation.isformatofVersió postprint del document publicat a: https://doi.org/10.1007/s10870-010-9960-y
dc.relation.ispartofJournal of Chemical Crystallography, 2011, vol. 41, p. 721-726
dc.relation.urihttps://doi.org/10.1007/s10870-010-9960-y
dc.rights(c) Springer Verlag, 2011
dc.rights.accessRightsinfo:eu-repo/semantics/openAccess
dc.sourceArticles publicats en revistes (Mineralogia, Petrologia i Geologia Aplicada)
dc.subject.classificationEstructura cristal·lina (Sòlids)
dc.subject.classificationCristal·lografia
dc.subject.otherLayer structure (Solids)
dc.subject.otherCrystallography
dc.titleSynthesis, Structural Characterization and Spectroscopic Properties of 1,2-Bis[4-(3,5-dimethyl-1H-pyrazol-1-yl)-2-oxobutyl]benzene
dc.typeinfo:eu-repo/semantics/article
dc.typeinfo:eu-repo/semantics/acceptedVersion

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