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2015-07-26

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Please use this identifier to cite or link to this item: https://hdl.handle.net/2445/138570

Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device

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https://doi.org/10.1007/s00723-015-0680-5

Abstract

Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system.

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Espectroscòpia de ressonància magnètica nuclear, Polarització (Física nuclear)

Subject (English)

Nuclear magnetic resonance spectroscopy, Polarization (Nuclear physics)

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Articles publicats en revistes (Química Inorgànica i Orgànica)
Publicacions de projectes de recerca finançats per la UE

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KATSIKIS, Sotirios, et al. Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device. Applied Magnetic Resonance. 2015. Vol. 46, num. 7, pags. 723-729. ISSN 0937-9347. [consulted: 12 of June of 2026]. Available at: https://hdl.handle.net/2445/138570

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