Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device

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dc.contributor.authorKatsikis, Sotirios
dc.contributor.authorMarín Montesinos, Ildefonso
dc.contributor.authorPons Vallès, Miquel
dc.contributor.authorLudwig, Christian
dc.contributor.authorGünther, Ulrich L.
dc.date.accessioned2019-07-30T10:38:27Z
dc.date.available2019-07-30T10:38:27Z
dc.date.issued2015-07-26
dc.date.updated2019-07-30T10:38:27Z
dc.description.abstractDissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system.
dc.format.extent7 p.
dc.format.mimetypeapplication/pdf
dc.identifier.idgrec655715
dc.identifier.issn0937-9347
dc.identifier.urihttps://hdl.handle.net/2445/138570
dc.language.isoeng
dc.publisherSpringer Verlag
dc.relation.isformatofVersió postprint del document publicat a: https://doi.org/10.1007/s00723-015-0680-5
dc.relation.ispartofApplied Magnetic Resonance, 2015, vol. 46, num. 7, p. 723-729
dc.relation.projectID info:eu-repo/grantAgreement/EC/FP7/261863/EU//BIO-NMR
dc.relation.urihttps://doi.org/10.1007/s00723-015-0680-5
dc.rights(c) Springer Verlag, 2015
dc.rights.accessRightsinfo:eu-repo/semantics/openAccess
dc.sourceArticles publicats en revistes (Química Inorgànica i Orgànica)
dc.subject.classificationEspectroscòpia de ressonància magnètica nuclear
dc.subject.classificationPolarització (Física nuclear)
dc.subject.otherNuclear magnetic resonance spectroscopy
dc.subject.otherPolarization (Nuclear physics)
dc.titleImproved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
dc.typeinfo:eu-repo/semantics/article
dc.typeinfo:eu-repo/semantics/acceptedVersion

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